Добавил:
kiopkiopkiop18@yandex.ru Вовсе не секретарь, но почту проверяю Опубликованный материал нарушает ваши авторские права? Сообщите нам.
Вуз: Предмет: Файл:

6 курс / Диетология и нутрициология / ОСТАТОЧНЫЕ_СОДЕРЖАНИЯ_ПЕСТИЦИДОВ_В_ПИЩЕВЫХ_ПРОДУКТАХ_МЕТОДЫ

.pdf
Скачиваний:
1
Добавлен:
24.03.2024
Размер:
670.28 Кб
Скачать

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

Номер

Соединение

Ссылки

ККОП

 

 

(CCPR)

 

 

136

Процимдион

2a,.2d,.4.(XII-6;.S8,.S19),.7a.(6),.7c.

 

 

(S8,.S19),.10.

137

Бендиокарб

2d,.2g,.6d,.4.(XII-6),.7a.(6),.9a.(M2,.

 

 

M13).Ambrus.

138

metalaxyl

2c,.2d,.2e,.4.(XII-6;.S8,.S19;.517),.7a.

 

 

(6),.7b,.7c.(S19),9a.(M4),.10.Ambrus .

139

Бутакарбоксим

2g,.9a.(M13).Aharonson,.Brauckhoff,.

 

 

Li,.Muszkat.

140

Нитрофен

1a,.2a,.2d,.2e,.4.(XII-6;.S19;.340),.6d,.

 

 

7a.(6),.7b,.7c.(S19) .Adler,.Ambrus,.Yu .

141

Фоксим

2d,. 4. (XII-6;. S19;. 307),. 7a. (6),. 7c.

 

 

(S19),.9a.(M2,.M12) .Ambrus

142

Прохлораз

2d .Maclaine.Pont,.Somerville .

143

Триазофос

2c,.2d,.4.(XII-4,6;.S8,.S19;.401),.6d,.

 

 

7a.(6),.7c.(S19),.9a(M2,.M5,.M12),.10.

 

 

Ambrus

144

Битетранол

2d,. 4. (XII-6;. S19;. 613;. 613A),. 7a.

 

 

(6),.7c.(S19),.7d.(613A,.426,.605),.9a.

 

 

(M12).Brennecke.(1,3) .

145

Карбосульфан

2d,.4.(658.-.(344)).Leppert.(1,2) .

146

Цигалотрин

2d,.6g .

147

Метопрен

2e,.6d .

148

Пропамокарб

Gentile .

149

Этопрофос

2c,.2d,.2e,.4.(XII-6;.S8,.S19),.7a.(6),.

 

 

7b,.7c.(S19),.9a.(M2,.M5).Ambrus

150

Пропилен.тиомочевина

Lembo,.Nitz

151

Диметипин

2e.

152

Флуцитринат

2d,.2e.

153

Пиразофос

2d,.4.(XII-4,6;.S8,.S19;.328),.6d,.7a.(6),.

 

 

7b,.7c.(S19),.9a.(M2,.M5,.M12),.10.

154

Тиодикарб

2g.

155

Беналаксил

.4.(S19).not.published.yet.

156

Клофентизин

Bichi,.Snowdon.

157

Цифлутрин

2d,.4.(S23),.9a.(M11).

158

Глифосат

2e,. 4. (405),. 6h,. 7d. (405). 9b. Cowell,.

 

 

Tuinstra,.Wigfield.

159

Винклозолин

2a,. 2d,. 4. (XII-6;. S8,. S19;. 412),. 9a.

 

 

(M1,.M12).

 

 

Раздел.2. .Список.методов.анализа

 

 

 

 

Номер

Соединение

Ссылки

ККОП

 

 

 

(CCPR)

 

 

 

160

Пропиконазол

2d,.4.(S19;.624),.7d.(624).

161

Паклобутразол

2d.Reed.

162

Толилфлуанид

2d,. 4. (XII-6;. S. 8;. S19:. 371;. 203-.

 

 

(371)),.7c.(S8,.S19),.7d.(203A,371A).

 

 

9a. (M1,M12). Brennecke. (4). Specht.

 

 

(2),.Anderson.

163

Анилазин

4.(XII-6;.S19:.186),.7c.(S19),.7d.(186).

 

 

2d,.2e.Lawrence(2),.Brennecke(5).

164

Деметон-S-метилсульфон

4(XII-6,.S16,.S19),.7c.(S16),.9a.(M5),.

 

 

2d,.2e .Andersson,.Thornton,.Wagner .

165

Флузилазол

2d,.4(S19)(only.parent.compound).

166

Метил-оксимедон

4(XII-6,.S16,.S19),.7c.(S16),.9a.(M5),.

 

 

2c,.2d,.2e .Thornton,.Wagner .

167

Тербуфоз

4. (S8;. S19),. 9a(M5). (Only. parent.

 

 

compound),.2c,.2d,.2e .Westcott .

168

Триадименол

4.(XII-6,.S19,.425.-.(605)).7a.(6),.7c.

 

 

(S19),. 9a. (M12),. 2d . Allmendinger,.

 

 

Andersson,. Brennecke. (2),. Ragab,.

 

 

Mendes.

169

Циромазин

2e.Cabras,.Bardalaye.

170

Гексаконазол

2d,.11.

171

Профенофос

2c,.2d,.2e.Andersson.

172

Бентазон

2e.Cessna,.Hogendoorn.

173

Бупрофезин

Nishizawa. JAOAC. accepted. for.

 

 

publication,.Ishii.(1).

174

Кадузафос

2d.

175

Глуфосинат.аммония

4.(651),.7d.(651) .

176

Гексатиазокс

2e.

177

Абамектин

2e.Prabhu,.Vuik .

178

Бифентрин

2a,2e .

179

Циклоксидин

 

 

180

Дитианон

Baker,.Kadenczki .

181

Миклобутанил

2e.

182

Пенконазол

2d.

183

Профам

2d,.4.(s11),.6e.(343-350).7c.(S11).

184

Этофенпрокс

 

 

185

Фенпропатрин

2,.7d.(S23).Nakamura .

76

77

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

Номер

Соединение

Ссылки

ККОП

 

 

(CCPR)

 

 

186

Метирам

see.105:.dithiocarbamates .

187

Клетодим

 

188

Фенпропиморф

Kadenczki,. v. . Zoonen,. Dieckmann,.

 

 

Lafuente.(1,2),.Tadeo

189

Тебуконазол

7c(S19).Brennecke.(6),.Allmendinger,.

 

 

Maasfeld

190

Тефлубенурон

 

191

Метил-толклофос

4.(s19),.7a.(6),.7c.(s19),.7d.(S8).Becker,.

 

 

Ishii,.Stan,.Philips .

РАЗДЕЛ 3. СПРАВОЧНАЯ ЛИТЕРАТУРА

3.1. ОСНОВНЫЕ СТАТЬИ

В. приведенных. ниже. документах. или. книгах. рассматриваются. общие. проблемы.анализа.остаточных.содержаний.пестицидов.(также.см.. руководства.в.пар. .3..2):

Ambrus,.A. .&.Thier,.H..-P..,.Application.of.multi-residue.procedures.in.pesticides. residues.analysis,.Pure.Appl. .Chem..,.58,.1035-1062.(1986). .

Beck,. H..,. Untersuchungsmethoden. zur. Bestimmung. der. Rьckstдnde. von. Chlorkohlenwasserstoff-Pestiziden. in. oder. auf. Lebensmitteln,. Bundesgesundheitsblatt,.17,.269-274.(1974)..

Becker,.G. .et.al..,.Dьnnschichtchromatographie.in.der.Rьckstandsanalytik.von. Pflanzenschutzmitteln. und. deren. Metaboliten,. Verlag. Chemie. VCH,. Weinheim,.FRG .(1987)..

Burke,.J..A..,.The.interlaboratory.study.in.pesticide.residue.analyses,.in:.Advances. in.Pesticide.Science,.H. .Geissbuehler.(edit..),.Pergamon.Press,.Oxford,. UK,.633-642.(1979). ..

Carl,.M..,.Internal.laboratory.quality.control.in.the.routine.determination.of. chlorinatedpesticides,.in:.Advances.in.Pesticide.Science,.H. . Geissbuehler. . (edit..),.Pergamon.Press,.Oxford,.UK,.660-663.(1979). .

Cochrane,.W..P..,.Chemical.derivatization.in.pesticide.analysis,.,.Plenum.Press,. New.York,.N..Y.., .USA,.(1981). .

Egli,.H..,.Storage.stability.of.pesticide.residues,.J. .Agr. .Fd. .Chem..,.30,.861-866. (1982).

Frehse,.H. .&.Timme,.G..,.Quantitative.residue.analytical.reliability:.beatitude. through.the.application.of.latitude,.Res. .Revs..,.73,.27-47.(1980). .

Gunther,.F..A..,.Interpreting.pesticide.residue.data.at.the.analytical.level,.Res. .

Revs..,.76,.155-171.(1980). .

Раздел.3. .Справочная.литература

Horwitz,.W..,.The.role.of.the.analyst.in.analytical.chemistry,.FDA.Bylines,.4,. 169-178.(1979). .

Horwitz,.W..,.The.inevitability.of.variability.in.pesticide.residue.analysis,.in:. Advances. in. Pesticide. Science,. ,. H. . Geissbuehler. (edit..),. Pergamon. Press,.Oxford,.UK,.649-655.(1979). .

Horwitz,. W. . et. al..,. Quality. assurance. in. the. analysis. of. foods. for. trace. constituents,.AOAC,.63,.1344-1354.(1980). .

Horwitz,.W..,.Evaluation.of.analytical.methods.used.for.regulation.of.foods.and. drugs, .Anal. .Chem..,.54,.67A-76A.(1982). .

ISO. Document. ISO. 5725,. 2nd. edit. . (1986),. Precision. of. test. methods:. determination.of.repeatability.and.reproducibility,.ISO.Recomendation. 5725,.2th.edition.(1986).

IUPAC.Reports.on.Pesticides.(13),.Development.and.evaluation.of.simplified. approaches. to. residues. analysis,. Pure. Appl. . Chem..,. 53,. 1039-1049. (1981)..

Moye,.H..A. .(edit..),.Analysis.of.pesticide.residues,.Vol. .58.of:.Chemical.Analysis,. John.Wiley.and.Sons,.New.York,.N..Y..,.USA.(1981). .

Pesticide. Residue. Analysis,. Health. Aspects. of. Chemical. Safety,. ,. Interim. Document. 14,. WHO,. Regional. Office. for. Europe,. Copenhagen,. Denmark.(1984). .

Safe,.S. .&.Hutzinger,.O..,.Mass.spectrometry.of.pesticides.and.pollutants,.CFC. Press.Inc..,.Boca.Raton,.Florida,.USA .(1979). .

Steiner,. E..H..,. Planning. and. analysis. of. results. of. collaborative. tests,. in:. Statistical.Manual.of.the.AOAC,.Washington,.D..C..,.USA.(1974). .

The.Agrochemical.Handbook,.The.Royal.Society.of.Chemistry,.The.University,. Nottingham,.UK,.(1983). .

Thier,. H..-P. . &. Frehse,. H..,. Rьckstandsanalytik. von. Pflanzenschutzmitteln,. Georg.Thieme.Verlag,.Stuttgart.-.New.York.(1986). .

Youden,. W..J..,. Statistical. techniques. for. collaborative. tests,. in:. Statistical. Manual.of.the.AOAC,.Washington,.D..C..,.USA.(1974). .

Zweig,.G. .(edit..),.Analytical.methods.for.pesticides,.plant.growth.regulators.and. food.additives,.Academic.Press,.New.York.-.San.Francisco.-.London,. Vol. .XIV.and.XV.(1986). .

3.2. РУКОВОДСТВА

(1). Официальные.методы.AOAC.INTERNATIONAL.(Official.Methods. of.AOAC.INTERNATIONAL,.16th.edition,.1995).

(a). 970..52

(b).976..23

(d). 977..18

(e). 975..40

(j). 978..16

(k). 977..19

(l). 960..43

78

79

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

(m). 963..24

(n). 983..21

(o). 984..21

(p). 985..22

(q). 985..23

(2). Аналитическое. руководство. по. пестицидам. (АРП). (Pesticide. Analytical. Manual),. Администрация. по. контролю. за. продуктами. питания. и. лекарствами,. Вашингтон,. федеральный. округ. Колумбия,.США

2-ая редакция

3-я редакция

aТом. .I Таблица.201-A.и.разделы,. Нежирные. продукты:.

211..1,. 212..1,. 231..1,. 232..1. Раздел.303

и.252 Жирные. продукты:.

Раздел. 304,. E1-E5+C1- C4

bТом. .I Таблица.201-D.и.раздел. Раздел.402

221..1.

cТом. .I Таблица.201-H.и.раздел. 3.[метода.нет.в.PAM.I.3-е.

232.. издание]

dТом. .I Таблица. 201-I. и. раздел. Раздел. 302. E1-E4,. не.

232..4. сброшен

eТом. .II Меьлж. по. индефикаци-

онному.номеру.(в.случае. ссылки. на. ряд. методов,. они. указываются. в.порядке. предпочтительности)

fТом. .I Таблица.651-A.и.разделы. [нет. в. PAM. I. 3-е. изда-

650.и.651

ние]

gТом. .I Таблица.242..2-1.и.раздел. Раздел.401

242..2.

h

Том. .I, Раздел .242..3.

Раздел.404

(3). Manual.on.Analytical.Methods.for.Pesticide.Residues.in.Foods,.Health. Protection.Branch,.Health.and.Welfare.Canada,.Ottawa,.Ont..,.Canada. (1985).(available.in.English.and.French).

(4). Methodensammlungzur.R.ьckstandsanalytikvon.Pflanzenschutzmitteln,. . 1..-. 11. . Lieferung,. VCH. Verlagsgesellschaft,. Weinheim,. FRG. (1991). (the.numbers.in.parentheses.refer.to.the.numbers.of.the.methods.in.this. manual;. methods. preceeded. by. “S”. are. multi-residue. methods;. .the. manual.is.also.available.in.English,.see.ref. .7).(4)Methodensammlung.

Раздел.9Раздел. .М тоды.3. .Справочная.анализа.и.отбора.литература.проб

zur.Rьckstandsanalytik.von.Pflanzenschutzmitteln,.1..-.11. .Lieferung,. VCH.Verlagsgesellschaft,.Weinheim,.FRG.(1991).

(5). Laboratory. Manual. for. Pesticide. Residues. Analysis. in. Agricultural. Products,. compiled. by. R..B. . Maybury,. Pesticide. Laboratory,. Food. Production.and.Inspection.Branch,.Agriculture.Canada,.Ottawa,.Ont..,. Canada.(1984).(available.in.English.and.French). .

(6). Zweig,. G. . (edit..),. Analytical. Methods. for. Pesticides,. Plant. Growth. Regulators.,.Academic.Press,.New.York.-.San.Francisco.–.London.(6). Zweig,.G. .(ред..),.

(a). Vol. .VII.(1974)

(b). Vol. .VIII.(1976)

(c). Vol. .IX.(1977)

(d). Vol. .X.(1978)

(e). Vol. .XI.(1980)

(f). Vol. .XII.(1982).(Lawrence.J..F. .Editor)

(g). Vol. .XIII.(1984).(Zweig,.G. .and.Sherma,.J. .Editors)

(h). Vol. .XVI.(1988).(Sherma,.J. .Editor)

(7). Manualof.Pesticide.Residue.Analysis,.Deutsche.Forschungsgemeinschaft,. . VCH.Verlagsgesell-.schaft,.Weinheim,.FRG.(1987).(English.translation. of.ref. .4).

(a). Vol. .I,.Section.Clean-up.Methods.(the.numbers.in.parentheses. refer.to.the.numbers.of.the.clean-up.methods.in.this.volume).

(b). Vol. .I,.Section.Individual.Pesticide.Residue.Analytical.Methods.

(c). Vol. .I,.Section.Multiple.Pesticide.Residue.Analytical.Methods. (the.numbers.in.parentheses.refer.to.the.numbers.of.the.multiresidue.methods.in.this.volume)..

(d). Vol. .II.(1992). .Том.II.(1992)..

(8). Chemistry. Laboratory. Guidebook,. United. States. Department. of. Agriculture,. Food. Safety. and. Inspection. Service,. Science. Program,. Washington,.D..C..,.USA.

(a). Section.5..001

(b). Section.5..002

(c). Section.5..003

(d). Section.5..004

(e). Section.5..006

(f). Section.5..005

(g). Section.5..050

(9). Analytical. Methods. for. Residues. of. Pesticides. in. Foodstuffs,. P..A. . Greve.(edit..),.5th.edition,.Government.Publishing.Office,.The.Hague,. Netherlands.(1988).

80

81

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

(a). Part.I:.Multi-residue.Methods.(the.numbers.in.parentheses.refer. to.numbers.of.the.multi-residue.methods.in.this.volume).

(b). Part.II:.Special.Methods.(methods.given.under.compound.name).

Часть.II:.

(10). Materials. and. Methods. Used. for. Pesticide. Residues. Monitoring. in. Sweden,.Vеr.Fцda,.38,.Suppl..2,.79-136.(1986).

(11). Comprehensive. Analytical. Profiles. of. Important. Pesticides. (Modern. methods.for.pesticides.analysis).e..d. .J. .Sherma.&.T.Cairns.1992. .

3.3.ОТДЕЛЬНЫЕ ДОКУМЕНТЫ

Номера,.выделенные.курсивом.после.ссылок,.соответствуют.соединениям,. обозначенным. по. их. номеру. ККОП,. к. которому. применяются. включенные.методы..

Abbott.(1),.D..C. .et.al..,.Pest. .Sci..,.1,.10-13.(1970).Pesticide.residues.in .the. total.diet.in.England.and.Wales,.1966-1967;.Part.III:.Organophosphorus. pesticide.residues.in.the.total.diet.

2, 4, 5, 11, 14, 22, 25, 27, 28, 34, 36, 37, 39, 42, 49, 53, 55, 58, 59, 60, 66, 68, 73, 74, 76, 92, 112, 124

Abbott.(2),.D..C. .et.al..,.J. .Chromatog..,.16,.481-487.(1964) .Some.observations. on.the.thin-layer.chromatography.of.organochlorine.pesticides

1, 21, 32, 33, 43, 48

Adachi,.K. .et.al..,.JAOAC,.67,.798-800.(1984).Simple.analytical.method.for. organophosphorus.pesticide.determination.in.unpolished.rice,.using .removal.of.fats.by.zinc.acetate

.22,.27,.37,.49,.58,.128.

Adler,.I..L. .&.Wargo.Jr,.J..P..,.JAOAC,.58,.551-553.(1975) .Determination.of. residues.from.the.herbicide.2,4-dichloro-1-(4-nitrophenoxy)-benzene. in.rice.and .wheat.by.electron-capture.gas-liquid.chromatography

140

Aharonson,.N. .&.Muszkat,.L..,.Z. .Lebensm. .Unters. .Forsch..,.180,.96-100.(1985). Direct.gas.chromatographic.determination.of.the.two.isomeric.insecticides,.aldicarb.and.butocarboxime.and.their.toxic.metabolites:.application.to.residue.analysis.in.crops.and.leaves

117, 139

Allen.(1),.J..G. .&.Hall,.K..J..,.J. .Agr. .Fd. .Chem..,.28,.255-258.(1980).Methods.for. the.determination.of.diphenylamine.residues.in.apples

30

Allen.(2),.J..G..,.Pest. .Sci..,.11,.347-350.(1980).Daminozide.residues.in.sweet. cherries,.and.their.determination.by.colorimetric.and.gas-liquid.chro- matographic.methods

104

Раздел.3. .Справочная.литература

Allmendinger,.H. .Pflanzensch. .Nachr. .Bayer,.44,.5-66.(1991).A.method.for. determining.residues.of.the.fungicides.folicur.and.Bayfidan.in.plant.material.and.soil.by.gas.chromatography..

168, 189

Ambrus,.A. .et.al..,.JAOAC,.64,.733-768.(1981) .General.method.for.determina- tion.of.pesticide.residues.in.samples.of.plant.origin,.soil,.and.water

1, 2, 4, 6, 7, 8, 14, 17, 21, 22, 25, 27, 32, 33, 37, 39, 41, 42, 43, 48, 49, 51, 53, 54, 58, 59, 60, 61, 66, 72, 73, 74, 75, 76, 77, 80, 81, 82, 83, 86, 87, 94, 96, 101, 103, 112, 113, 117, 118, 119, 120, 123, 128, 133, 135, 137, 140, 141, 143, 159

Andersson,.A.and.Ohlin,.B. .Vеr.Fцda.38,.79-109.(1986).A.capillary.gaschro- matographic.multiresidue.method.for.the.determination.pesticide.resi-

dues.in.fruit.and.vegetables..

 

162, 164, 168,

171

 

Austin,.D..J. .&.Hall,.K..J..,.Pest. .Sci..,.12,.495-502.(1981) .A.method.of.analysis.

for.the.determination.of.binapacryl,.bupirimate.and.diflubenzuron.on.

apple.foliage.and.fruit,.and.its.application.to.persistence.studies .

3, 130

 

 

Baker,.P..B. .(1).&.Flaherty,.B..,.Analyst,.97,.713-718.(1972) .Fungicide.residues;.

Part.II:.The.simultaneous.determination.of.residues.of.folpet,.captan.and.

captafol.in.selected.fruits.by.gas.chromatography.

6, 7, 41

 

 

Baker,.P..B. .(2).&.Hoodless,.R..A..,.Analyst,.98,.172-175.(1973) .Fungicide.resi-

dues;.Part.III:.The.determination.of.binapacryl.in.selected.fruits.by.gas.

chromatography

 

3

 

 

Baker,.P..G. .(1).et.al..,.Analyst,.105,.282-285.(1980).Fungicide.residues;.Part.

VII:.Determination.of.residues.of.fentin.in.vegetables.and.cocoa.prod-

ucts.by.spectrofluorimetry.

 

40

 

 

Baker,.P..G. .(2).&.Bottomley,.P..,.Analyst,.107,.206-212.(1982).Determination.

of.residues.of.synthetic.pyrethroids.in.fruit.and.vegetables.by.gas-liquid.

and.high-performance.liquid.chromatography.

93, 118, 119, 120, 127, 135

 

Baker,.P..G. .&.Clarke,.P..G..,.Analyst.109,.81-83.(1984) .Determination.of.residues.

of.dithianon.in.apples.by.HPLC .Bardalaye,.C,.Wheeler,.W..B. .&.Meister.

C..W. .JAOAC.70,.455-457.(1987).Gas.chromatographic.determination.of.

cyromazine.and.its.degradation.product.melamine.in.chinese .cabbage. .

169

 

 

Becker,.G..,.Schug,.P..,.Deutsche.Lebensm. .Rundschau.86,.239-242.(1990).Eine.

miniaturmethode.zur.schnellen.Bestimmung.von.Pestizidrьckstдnden.in.

pflanzlichen.Lebensmitteln. ..

191

Bichi,.C. .et.al. .Pestic. .Sci. .30,.13-19.(1990).Simultaneous.determination.of.clofen- tezine,.fenoxycarb.and.hexthiazox.by.HPLC.on.apples,.pears.and.their.pulps.

156

82

83

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

Bottomley,.P. .&.Baker,.P..G..,.Analyst,.109,.85-90.(1984) .Multi-residue.de- termination. of. organochlorine,. organophosphorus. and. synthetic. py- rethroid.pesticides.in.grain.by.gas-liquid.and.high-performance.liquid. chromatography

1, 4, 21, 22, 25, 37, 44, 49, 61, 66, 86, 90, 93, 118, 119, 120, 123, 127, 135

Bourke,.J..B. .et.al..,.J. .Agr. .Fd. .Chem..,.25,.36-39.(1977).Residues.and.disap- pearance.of.triforine.from.various.crops .

116

Brauckhoff,.S. .&.Thier,.H..-P..,.Z. .Lebensm. .Unters. .Forsch..,.184,.91-95.(1987). Analysenmethode.fьr.Rьckstдnde.von.Methylcarbamat-Insecticiden.in. pflanzlichen.Lebensmitteln .

8, 75, 94, 96, 101, 107, 117, 132, 134, 137, 139

Brennecke. (1),. R..,. Pflanzensch. . Nachr. . Bayer,. (Engl. . edit..)38,. 33-54. (1985). Method. for. gas-chromatographic. determination. of. residues. of. Baycor. fungicide.in.plant.material,.soil.and.water.(Engl. .edit..:.38,.33-54.(1985)).

144

 

 

Brennecke(2),.R. ..,Pflanzensch. .Nachr. .Bayer,.37,.68.-93(1984).

Method.for.gas.-chro-

matographicdetermination.of.residues.of.Bayleton.and.Bayfidan.fungicides.in. .

plant.material,.soil.and.water.(German.edit..:.37,.66-91.(1984)) .

133, 168

 

 

Brennecke.(3),.R..,.Pflanzensch. .Nachr. .Bayer.,.41,.113-131.(1988).Method.for.

the.determination.of.residues.of.the.fungicide.Baycor.in.plant.material.

and.beverages.by.high.pressure.liquid.chromatography.with.fluorescence.

detection.(German.edit..:.41,.113-135.(1988)).

 

144

 

 

Brennecke.(4), .R..,.Pflanzensch. .Nachr. .Bayer,.41,.137-174.(1988). ..A.method.

for.the.determination.of.residues.of.the.fungicides.Euparen.and.Euparen.

M.in.plant .material.and.beverages.by.gaschromatography.(German.edit. .

41,.136-172.(1988)). ..

 

 

82, 162

 

 

Brennecke.(5), .R..,.Pflanzensch. .Nachr. .Bayer,.38,.11-32.(1985).Method.for.

gas-chromatographic.determination.of.Dyrene.residues.in.plant.mate-

rial,.soil.and.water .(German.edit..:.38,.11-32.(1985)). ..

163

 

 

Brennecke.(6), .R..,.Pflanzensch. .Nachr. .Bayer,.42,.223-284.(1989).German.edit. .

A.method.for.determining.residues.of.the.fungicides.Euparen,.Euparen.

M.and.Folicur.in.plant.material.and.beverages.by.gaschromatography. .

189

 

 

Buettler,.B. .&.Hoermann,.W..D..,.J. .Agr. .Fd. .Chem..,.29,.257-260.(1981).High-

pressure.liquid.chromatographic.determination.of.captan,.captafol,.and.

folpet.residues.in.plant.material.

 

 

6, 7, 41

 

 

Cabras,. P..,. Meloni,. M..,. &. Spaneddal,. J. . Chromatogr. . 505,. 413-416. (1990).

High-performance. liquid. chromatographic. separation. of. cyromazine.

and.its.metabolite.melamine. .

169

 

Раздел.3. .Справочная.литература

Calderbank.(1),.A. .&.Yuen,.S..H..,.Analyst,.90,.99-106.(1965).An.ion-exchange. method.for.determining.paraquat.residues.in.food.crops .

57

Calderbank.(2),.A. .&.Yuen,.S..H..,.Analyst,.91,.625-629.(1966).An.improved. method.for.determining.residues.of.diquat .

31

Cessna,.A..J. .J..Agr..Fd..Chem. .33,.108-110.(1985) .Gas.chromatograohic.analy- sis.of.the.herbicide.bentazone.in.leeks.

172

Chaput,.D. .JAOAC,.71,.542-546,.(1988).Simplified.multiresidue.method.for. liquid.chromatographic.determination.of.N-methylcarbamate.insecti- cides.in.fruits.and.vegetables. .

8, 75, 94, 96, 117, 132

Cochrane,.W..P. .et.al..,.JAOAC,.59,.617-621.(1976).Gas-liquid.chromatographic. analysis.of.ethephon.and.fenoprop.residues.in.apples.and.their.decline. before.and.after.harvest .

106

Conditt,.M.et.al,.JAOAC,.71,.735-739.(1988). .Gas.chromatography/mass.spec- trometric.determination.of.daminozide.in.high.protein.food.products. .

104

Cowell,.J..E..,.Kunstman,.J..L..,.Nord,.P..J..,.Steinmetz,.J..R. .and.Wilson,.G..R. .J. . Agric. .Fd. .Chem. .34,.955-960.(1986) .Validation.of.an.analytical.method. for.analysis.of.glyphosate.and.Metabolite:.An.interlaboratory.study.

158

Daft,.J..L..,.JAOAC,.66,.228.(1983) .Gas.chromatographic.determination.of.fumigant.residues.in.stored.grains,.using.isooctane .partitioning.and.dual. column.packings.

10, 23, 24

Day,.E..W. .et.al..,.JAOAC,.51,.39-44.(1968).Determination.of.sec-butylamine. residues.in.fruit .

89

Desmarchelier,. J. . et. al..,. Pest. . Sci..,. 8,. 473-483. (1977). A. collaborative. study. of.residues.on.wheat.of.chlorpyrifos-methyl,.fenitrothion,.malathion,. methacrifos.and.pirimiphos-methyl .

37, 49, 86, 90, 125

DieckmannH. . et.al,.Fresenius.J. . Anal. . Chem. . 345,.784.-786(1993). Simultaneous. . determination.of.fenpropimorph.and.the.corresponding.metabolite.fenpropimorphic.acid.in.soil. .

188

Ebing,. W. . et. al..,. Lebensm. . gerichtl. . Chem..,. 39,. 126-130. (1985). Zur. Rьckstandsanalytik. von. Phenoxyalkancarbonsдure-Herbiziden. in. Getreidekцrnern .

20, 121

Farrow,.J..E. .et.al..,.Analyst,.102,.752-758.(1977) .Fungicide.residues;.Part.VI:. Determination.of.residues.of.post-harvest.fungicides.on.citrus.fruit.by.

84

85

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

high-performance.liquid.chromatography.

29, 56, 65, 72

Francoeur,.Y. .&.Mallet,.V..,.JAOAC,.59,.172-173.(1976) .Determination.of. quinomethionate. (6-methylquinoline-2,3-diyldithiocarbamate). residues.in.crops.by.in.situ.fluorimetry.

80

Galoux,.M. .et.al..,.JAOAC,.65,.24-27.(1982) .Colorimetric.determination.of. 3-amino-1,2,4-triazole.in.grain.or.meal ..

79

Gentile,.I..A. .&.Passera,.E..,.J. .Chromatog..,.236,.254-257.(1982).Separation. and.detection.of.propamocarb.by.thin-layer.chromatography.

148

Gilvydis,.D..M. .&.Walters,.S..M..,.JAOAC,.67,.909-912.(1984) .Determination. of.captan,.folpet,.and.captafol.in.fruits.and.vegetables,.using.two.multiresidue.methods.

6, 7, 41

Heikes,.D..L..,.JAOAC,.68,.431-436.(1985).Purge.and.trap.method.for.determi- nation.of.ethylene.dibromide.in.table-ready.foods.

23

Hill,.A..R..C. .et.al..,.Analyst,.109,.483-487.(1984).Organophosphorus.sulphides,. sulphoxides.and.sulphones;.Part.I:.Determination.of.residues.in.fruit. and.vegetables.by.gas-liquid.chromatography

38, 39, 73, 74, 76, 85, 112

Hirvi,.T. .et.al..,.J. .Agr. .Fd. .Chem..,.27,.194-195.(1979).A.glass.capillary.gas-liq- uid.chromatography.method.for.determining.ethylenethiourea.without. derivatization .

108

Hogendoorn,. E..A. . and. Goewie,. C..E. . J. . Chromatogr. . 475,. 432-441. (1989). Residue. analysis. of. the. herbicides. cyanizine. and. bentazone. in. sugar. maize.and.surface.water.using.high-performance.liquid.chromatography. and.an.on-line.clean-up.column-sitching.procedure.

172

Hunter,.K. .&.Lindsay,.D..,.Pest. .Sci..,.12,.319-324.(1981) .High-pressure.liquid. chromatographic.determination.of.sec-butylamine.residues.in.potatoes.

89

Ishii,.Y. .(1).et.al..,.J. .Pest. .Sci..,.15,.205-209.(1990).Clean.up.procedure.for.de- termination.of.pesticide.residues.in.crops.using.charcoal.-.Florisil.mini. column .

Ishii,.Y. .(2).et.al..,.J. .Pest. .Sci. .15,.231-236.(1990) .Residue.analysis.of.organo- chlorine.pesticides.by.GC.equipped.with.a.Hall.electrolytic.conductivity. detector.(Halogen.mode).

191

Kadenczki,.L..,.et.al,.JAOAC.75,.53-61.(1992) .Column.extraction.of.residues. of.several.pesticides.from.fruits.and.vegetables:.A.simple.multi .residue. analysis.method.188

Раздел.3. .Справочная.литература

Khan,. S..U..,. Bull. . Envir. . Cont. . Tox..,. 14,. 745-749. (1975). Determination. of. paraquat.residues.in.food.crops.by.gas.chromatography.

57

King,.R..R..,.J. .Agr. .Fd. .Chem..,.26,.1460-1463.(1978).Gas.chromatographic. determination.of.diquat.residues.in.potato.tubers .

31

Kitada,.Y. .et.al..,.JAOAC,.65,.1302-1304.(1982) .Simultaneous.liquid.chromato- graphic.determination.of.thiabendazole,.o-phenylphenol,.and.diphenyl. residues.in.citrus.fruits,.without.prior.cleanup.

29, 56, 65

Kobayashi,.H. .et.al..,.J. .Pest. .Sci..,.2,.427-430.(1977) .Gas.chromatographic. determination.of.guanidino.fungicide,.guazatine,.in.rice.grain.

114

Krause.(1),.R..T. .&.August,.E..M..,.JAOAC,.66,.1018-1022.(1983).Applicability. of.a.multiresidue.method.and.high.performance.liquid.chromatography. for.the.determination.of.chinomethionate.in.apples.and.oranges.

80

Krause.(2),.R..T. .&.August,.E..M..,.JAOAC,.66,.234-240.(1983).Applicability.of. a.carbamate.insecticide.multiresidue.method.for.determining.additional. types.of .pesticides.in.fruits.and.vegetables.

62

Lafuente.(1).M..T. .et.al,.JAOAC.69,.859-862.(1986).GC.determination.of.fen- propimorph.residues.in.citrus.fruit.

188

Lafuente.(2).M..T. .et.al,.Fres. .J. .Anal. .Chem. .328,.105-107.(1987).GLC.multi- residue.analysis.of.postharvest.fungicides.in.citrus.fruit.

188

Lane.(1),.J..R..,.JAOAC,.46,.261-268.(1963).Collaborative.study.of.maleic.hdra- zide.residue.analysis.

102

Lane.(2),.J..R..,.JAOAC,.48,.744-748.(1965).Collaborative.study.of.maleic.hy- drazide.residue.analysis.

102

Lawrence(1),.J..F..,.J. .Agr. .Fd. .Chem..,.25,.211-212.(1977) .Direct.analysis.of. some.carbamate.pesticides.in.foods.by.high-pressure.liquid.chromatog- raphy.

8, 75, 96

Lawrence. (2),. J..F. . &. Panopio,. L..G. . JAOAC. 63,. 1300-1303. (1980). Comparison. of. gas. and. liquid. chromatography. for. determination. of. anilazine.in.potatoes.and.tomatoes. ..

163

Lembo,.S. .et.al..,.J. .Chromatog..,.267,.427-430.(1983).Gas-liquid.chromato- graphic. method. for. determining. propylenethiourea. in. rat. tissues. and. fluids.

150

86

87

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

Leppert.(1),.B..C. .et.al..,.J. .Agr. .Fd. .Chem..,.31,.220-223.(1983).Determination. of.carbosulfan.and.carbofuran.residues.in.plants,.soil,.and.water.by.gas. chromatography

145

Leppert.(2),.B..C. .et.al..,.J. .Agr. .Fd. .Chem..,.32,.1441.(1984).Comment.on.recovery.of.carbosulfan.residues.from.acidic.crops.

145

Li.Yu-Chang.et.al..,.Fres. .Z. .Anal. .Chem..,.316,.290-292.(1983).Methode.zur. Bestimmung.von.Rьckstдnden.an.Butocarboxim.in.Pflanzen.und.Boden. mit.Hilfe.der.HPLC .

139

Lokke.(1),.H..,.J. .Chromatog..,.200,.234-237.(1980).Determination.of.amitrole. by.ion-pair.high-performance.liquid.chromatography.

79

Lokke.(2),.H..,.J. .Chromatog..,.179,.259-270.(1979).Investigation.on.loss.of. chlorothalonil,. dichlofluanid,. tolylfluanid. and. vinclozolin. by. column. chromatography.clean-up.on.silver-loaded.alumina.in.a.gas.chromato- graphic.multiresidue.procedure .

81, 82

Lokke.(3),.H. .&.Odgaard,.P..,.Pest. .Sci..,.12,.375-384.(1981).Residues.in.black- currants,.fodder.peas,.spinach.and.potatoes.treated.with.sublethal.doses. of.2,4,5-T.to.simulate.wind.drift.damage.

121

Lord,.E. .et.al..,.J. .Assoc. .Publ. .Anal..,.16,.25-32.(1978).The.determination.of. biphenyl.and.2-hydroxybiphenyl.in.citrus.fruit.

29, 56

Lott,.P..F. .et.al..,.J. .Chromat. .Sci..,.16,.390-395.(1978).The.determination.of. paraquat.

57

Love,.J..L. .&.Patterson,.J..E..,.JAOAC,.61,.627-628.(1978).Atomic.absorption. spectrometric.determination.of.cyhexatin .

67

Lubkowitz,.J..A. .et.al..,.J. .Agr. .Fd. .Chem..,.21,.143-144.(1973).Residue.studies.of. O,S-dimethyl.phosphoroamidothioate.on.tomatoes .

100

Luke,. B..G. . &. Cossens,. S..A..,. Bull. . Envir. . Cont. . Tox..,. 24,. 746-751. (1980). Determination.of.diphenylamine.residues.in.apples.

30

Maasfeld,.Pflanzenschutz.Nachr. .Bayer.40,.29-48.(1987).German.Ed. .Method.for. GC.determination.of.residues.of.the.fungicide.Folicur.in.plant.material.

189

Maclaine.Pont,.M..A. .et.al..,.Meded. .Fac. .Landbouww. .Rijksuniv. .Gent,.45,. 835-840.(1980).The.residue.analysis.of.prochloraz.in.combination.with. dicloran.

142

Раздел.3. .Справочная.литература

Mendes,.M..C..S. .J. .Agric. .Fd. .Chem. .38.174-178.(1990).Evaluation.and.confir- mation.of.acetylation.gas.liquid.chromatographic.method.for.the.determination.of.triadimenol.in.foods..

168

Mestres. (1),. R. . et. al..,. Trav. . Soc. . Pharm. . Montpellier,. 35,. 87-100. (1975). Mйthode.rapide.de.contrфle.et.de.dosage.des.rйsidus.d’ortho-phйnyl. phйnol.et.de.biphйnyle.dans.les .agrumes .

29, 56, 72, 77

Mestres.(2),.R. .et.al..,.Ann. .Fals. .Exp. .Chim..,.73,.407-420.(1980).Mйthode. de.recherche.et.de.dosage.des.rйsidus.de.pesticides.dans.les.produits. cйrйaliers;.2o: .Fumigants .

9, 10, 23, 24, 52

Mestres. (3),. R. . et. al..,. Proc. . Int. . Soc. . Citricult..,. 3,. 1103-1106. (1977). Thiophanate-methyl.postharvest.residues.in.oranges.

65, 72, 77

Moellhoff.(1),.E..,.Pflanzensch. .Nachr. .Bayer.(Engl. .edit..),.28,.370-381.(1975). Method.for.gas-chromatographic.determination.of.Curaterr.residues.in. plants.and.soil.samples.with .consideration.to.metabolites .

96

Moellhoff.(2),.E..,.Pflanzensch. .Nachr. .Bayer.(Engl. .edit..),.30,.249-263.(1977). Method. for. gas-chromatographic. determination. of. Peropal. acaricide. and.its.metabolites.in.plants,.soil,.water.and.laboratory.animal.chow .

67, 129

Muszkat,.L. .&.Aharonson,.N..,.J. .Chromat. .Sci..,.21,.411-414.(1983).GC/CI/ MS.analysis.of.aldicarb,.butocarboxime,.and.their.metabolites .

117, 139

Nakamura.et.al..,.J. .AOAC.76,.1348-1361.(1993) .Determination.of.pyrethroid. residues.in.vegetables,.fruits,.grains,.beans.and.green.tea. ..

185

Newsome.(1),.W..H..,.J. .Agr. .Fd. .Chem..,.24,.997-999.(1976) .A.gas-liquid.chro- matographic.method.for.the.determination.of.dodine.residues.in.foods .

84

Newsome.(2),.W..H..,.J. .Agr. .Fd. .Chem..,.22,.887-889.(1974) .A.method.for. determining. ethylenebis(dithiocarbamate). residues. on. food. crops. as. bis(trifluoroacetamido)-ethane .

105

Newsome. (3),. W..H..,. J. . Agr. . Fd. . Chem..,. 28,. 270-272. (1980). A.method.for.the.determination.of.maleic.hydrazide.and.its.b-D-gluco- side.in.foods.by.high-pressure .anion-exchange.liquid.chromatography.

102

Newsome.(4),.W..H..,.J. .Agr. .Fd. .Chem..,.30,.778-779.(1982) .Determination.of. triforine.in.fruit.crops.as.N,N’-bis(pentafluorobenzoyl)piperazine.

116

Newsome.(5),.W..H..,.J. .Agr. .Fd. .Chem..,.28,.319-321.(1980).Determination.of. daminozide.residues.on.foods.and.its.degradation.to.1,1-.dimethylhy-

88

89

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

drazine.by.cooking.

104

Nishizawa,.H..,.et.al,.JAOAC.accepted.for.publication .Simple.clean-up.proce- dure.for.residue.analysis.of.buprofezin.and.its.metabolites.in.crops.by.GC.

Nitz,.S. .et.al..,.J. .Agr. .Fd. .Chem..,.30,.593-596.(1982).A.capillary.gas-liquid. chromatographic. method. for. determination. of. ethylenethiourea. and. propylene .thiourea.in.hops,.beer,.and.grapes .

108, 150

Official.Gazette,.no. .4.of.the.Notification.issued.on.March.20,.1979,.by.the. Japan.Environment.Agency.Residue.analysis.of.cartap.hydrochloride.

97

Ott,.D..E. .&.Gunther,.F..A..,.JAOAC,.909-912.(1982) .Field.screening.method. for.above-tolerance.residues.of.dithiocarbamate.fungicides .

105

Otto,.S. .et.al..,.J. .Envir. .Sci. .Health,.Part.B,.12,.179-191.(1977) .A.new.gas. chromatographic.determination.of.ethylene.thiourea.residues.without. derivatization .

108

Panel.(1).of.the.Committee.for.Analytical.Methods.for.Residues.of.Pesticides. and.Veterinary.Products.in.Foodstuffs.of.the.Ministry.of.Agriculture,. Fisheries. and. Food,. Analyst,. 98,. 19-24. (1973). The. determination. of. malathion.and.dichlorvos.residues.in.grain.

25, 49

Panel.(2).of.the.Committee.for.Analytical.Methods.for.Residues.of.Pesticides. and.Veterinary.Products.in.Foodstuffs.of.the.Ministry.of.Agriculture,. Fisheries. and. Food,. Analyst,. 101,. 386-390. (1976). Determination. of. residues.of.inorganic.bromide.in.grain .

4

Panel.(3).of.the.Committee.for.Analytical.Methods.for.Residues.of.Pesticides. and.Veterinary.Products.in.Foodstuffs.of.the.Ministry.of.Agriculture,. Fisheries. and. Food,. Analyst,. 102,. 858-868. (1977). Determination. of. residues.of.organophosphorus.pesticides.in.fruits.and.vegetables.

2, 27, 49, 55, 58

Panel.(4).of.the.Committee.for.Analytical.Methods.for.Residues.of.Pesticides. and.Veterinary.Products.in.Foodstuffs.of.the.Ministry.of.Agriculture,. Fisheries.and.Food,.Analyst,.104,.425-433.(1979).Determination.of.or- ganochlorine.pesticides.in.animal.fats.and.eggs.

1, 21, 33, 44, 48

Panel.(5).of.the.Committee.for.Analytical.Methods.for.Residues.of.Pesticides. and.Veterinary.Products.in.Foodstuffs.of.the.Ministry.of.Agriculture,. Fisheries.and.Food,.Analyst,.99,.570-576.(1974).The.determination.of. residues.of.volatile.fumigants.in.grain.

10, 23

Panel.(6).of.the.Committee.for.Analytical.Methods.for.Residues.of.Pesticides. and.Veterinary.Products.in.Foodstuffs.of.the.Ministry.of.Agriculture,.

Раздел.3. .Справочная.литература

Fisheries.and.Food,.Analyst,.106,.782-787.(1981).Determination.of.resi- dues.of.dithiocarbamate.pesticides.in.foodstuffs.by.a.headspace.method.

105

Panel.(7).of.the.Committee.for.Analytical.Methods.for.Residues.of.Pesticides. and.Veterinary.Products.in.Foodstuffs.of.the.Ministry.of.Agriculture,. Fisheries.and.Food,.Analyst,.105,.515-517.(1980).Determination.of.a. range.of.organophosphorus.pesticide.residues.in.grain.

4, 22, 27, 37, 49, 74, 86, 112

Panel.(8).of.the.Committee.for.Analytical.Methods.for.Residues.of.Pesticides. and.Veterinary.Products.in.Foodstuffs.of.the.Ministry.of.Agriculture,. Fisheries.and.Food,.Analyst,.110,.765-768.(1985).Determination.of.a. range.of.organophosphorus.pesticide.residues.in.grain.

4, 27, 37, 49, 86, 90, 123, 125

Panel.(9).of.the.Committee.for.Analytical.Methods.for.Residues.of.Pesticides. and.Veterinary.Products.in.Foodstuffs.of.the.Ministry.of.Agriculture,. Fisheries.and.Food,.Analyst,.112,.1559-1563.(1987).Determination.of. ethylenethiourea.in.canned.fruits.and.vegetables.

108

Phillips,. A..J..L..,. Phytophylactica. 24. 289-292. (1992). . Bioassay. of. tolclofosmethyl.in.bean.seed. .

191

Player,.R..B. .&.Wood,.R..,.J. .Assoc. .Publ. .Anal..,.18,.109-117.(1980) .Methods.of. analysis.-.collaborative.studies;.Part.III:.Determination.of.biphenyl.and. 2-hydroxybiphenyl.in.citrus.fruit .

29, 56

van.der.Poll,.J..M..,.Vink,.M. .and.Quirijns,.J..K. .Chromatographia,.30,.155-158,. 1990. .Determination.of.amitrole.in.plant.tissues.and.sandy.soils.by.capillary.gaschromatography.with.alkali.flame.ionization.detection. .

79

Pomerantz,.I..H. .&.Ross,.R..,.JAOAC,.51,.1058-1062.(1968) .Captan.and.struc- turally.related.compounds:.thin.layer.and.gas-liquid.chromatography.

6, 7, 41

Prabhu,.S..V..,.Varsolona,.R..J..,.Welmer. .T..A. .,.Egan,.R..S. .and.Tway,.P..C. .J. .Agr. . Fd. .Chem. . .40,622-625.(1992) .Rapid.and.sensitive.high.performance. liquid.chromatographic.method.for.the.quantificxation.of .abamectine. and.its.delta.8,9.isomer. ..

177

Pyysalo,.H. .et.al..,.J. .Chromatog..,.168,.512-516.(1979) .Extraction.and.determi- nation.of.o-phenylphenol.and.biphenyl.in.citrus.fruits.and.apples .

29, 56

Ragab,. M..T..H. . Anderson,. M..G. . &. Johnston,. H..W. . . Bull. Envir. . Contam. . Toxicol. .44,.100-105.(1990).Residue.analysis.of.triadimefon,.triadime- nol.and.the.BAY.KWG1342.diol.and.BAY.KWG1323.hydroxylated.matabolites.in.winterweed. .

133, 168

90

91

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

Rains,.D..M. .&.Holder,.J..W..,.JAOAC,.64,.1252-1254.(1981).Ethylene.dibro- mide.residues.in.biscuits.and.commercial.flour .

23

Rajzman,.A..,.Analyst,.99,.120-127.(1974) .Determination.of.thiabendazole.in. citrus.fruits.by.ultraviolet.spectrophotometry.

65

Reed,.A..N..,.J. .Chromatogr. .438,.393-400.(1988) .Quantification.of.triazole.and. pyrimidine.plant.growth.retardants.

161

Rosenberg,. C. . &. Siltanen,. H..,. Bull. . Envir. . Cont. . Tox..,. 22,. 475-478. (1979). Residues.of.mancozeb.and.ethylenethiourea.in.grain.samples.

108

Roughan,.J..A. .et.al..,.Analyst,.108,.742-747.(1983).Modified.gas-liquid.chro- matographic.method.for.determining.bromide/total.bromine.in.foodstuffs .and.soils .

47

Sachse,. J..,. Z. . Lebensm. . Unters. . Forsch..,. 163,. 274-277. (1977). Ьber. die. Bestimmung.von.Chlorcholinchlorid.(CCC).in.Getreide.

15

Sano,. M. . et. al..,. JAOAC,. 62,. 764-768. (1979) . Flameless. atomic. absorption. spectrophotometric.determination.of.Vendex,.an.organic.tin.miticide,. in.apples,.oranges,.and.tea.leaves .

109

Saxton.W..L.et.al. .J. .Agric. .Food.Chem..,.37,.570-573.(1989) .Results.of.a.survey.for. the.presence.of.daminozide.and.unsymmetrical.dimethylhydrazine.in.food. .

104

Scudamore.(1),.K..A..,.Analyst,.105,.1171-1175.(1980).Determination.of.2-ami- nobutane.in.potatoes.using.high-performance.liquid.chromatography.

89

Scudamore(2),.K. ..A. &.Goodship,.G. ..,Pest. . Sci. ..,17,.385.-395(1986). Determination. . of.phosphine.residues.in.fumigated.cereals.and.other.foodstuffs.

46

Snowdon,.P..G..,.et.al,.Fresenius.J. .Anal. .Chem. .339,.444-447.(1991) .The.hy- drolysis.of.clofentazine.and.related.tetrazines.as.the.basis.of.determination.of.residues.in .bovine.tissues .

Somerville,.L..,.Meded. .Fac. .Landbouww. .Rijksuniv. .Gent,.45,.841-848.(1980). The.analysis.of.prochloraz.residues.in.cereals.

142

Specht.(1),.W. .&.Tillkes,.M..,.Fres. .Z. .Anal. .Chem..,.307,.257-264.(1981).Gas- chromatographische.Bestimmung.von.Rьckstдnden.von.Pflanzenbeha ndlungsmitteln.nach.Clean-up.ьber.Gel-Chromatographie.und.Mini- Kieselgel-Sдulen-Chromatographie;. 4. . Mitteilung:. Gas-chromatog- raphische.Bestimmung.von.11.herbiciden.Phenoxyalkancarbonsдuren. und.ihren.Estern.in.Pflanzenmaterial.

20, 121

Раздел.3. .Справочная.литература

Specht.(2),.W.and.Tilkes,.M,.Fres. .Z. .Anal. .Chem..,.322,.443-455.(1985). Gas-chromatographische.Bestimmung.von.Rьckstanden.von.Pflanze nbehandlungsmitteln.nach.Clean-up.ьber.Gel-Chromatographie.und. Mini-Kieselgel-Sдulen-Chromatographie,. V. . Methode. zur. aufarbeitung.von.Lebensmitteln.und.Futtermitteln.plantzlicher.und.tierischer. Herkunft.fьr.die.bestimmung.lipoid.und.wasserlцslicher.Pflanzenbeh andlungsmittel. .

162

Stan,.H..J..,.Heil,.S..,.Fresenius.J. .Anal,.Chem. .339,.34-39.(1991).Two.dimen- sional.capillary.gaschromatography.with.three.selective.detectors.as.a. valuable.tool.in.residue.analysis.—.State.of.the.art

191

Stijve.(1),.T..,.Deutsche.Lebensm. .Rundsch..,.77,.99-101.(1981).Gas.chromato- graphic.determination.of.inorganic.bromide.residues.—.a.simplified.pro- cedure.

47

Stijve(2),.T. ..,IUPAC.Pesticide.Chemistry,.Human.Welfare.and.the.Environment,. . J. .Miyamoto. (edit..),. Pergamon. Press,. Oxford,. UK,. 95-100. (1983). Miniaturised.methods.for.monitoring.organochlorine.pesticide.residues. in.milk .

1, 21, 43, 44, 48, 71

Stijve.(3),.T. .&.Brand,.E..,.Deutsche.Lebensm. .Rundsch..,.73,.41-43.(1977) .A. rapid,.low.cost,.small-scale.clean-up.method.for.the.determination.of. organochlorine.pesticide .residues.in.fats.and.oils .

1, 12, 21, 43, 44, 48

Stijve.(4),.T..,.Deutsche.Lebensm. .Rundsch..,.81,.321-322.(1985) .Inorganic. bromide.-.a.simple.method.for.the.confirmation.of.residue.identity.

47

Stijve.(5),.T..,.Deutsche.Lebensm. .Rundsch..,.76,.234-237.(1980) .Thin-layer.chro- matographic.determination.of.chlormequat.residues.in.various.substrates .

15

Stijve.(6),.T..,.Deutsche.Lebensm. .Rundsch..,.76,.119-122.(1980).The.determi- nation.of.bromopropylate.residues.

70

Stijve. (7),. T..,. Challenges. to. Contemporary. Dairy. Analytical. Techniques,. Royal.Society.of .Chemistry.(London),.Publ. .no. .49,.293-302.(1984). Determination.and.occurrence.of.organophosphorus.pesticide.residues. in.milk.

4, 14, 17, 18, 19, 22, 25, 27, 28, 34, 37, 49, 60, 86, 90

Tadeo,.J..L. .et.al,.J. .Chrom. .391,.338-342.(1987) .Determination.of.fenpropi- morph.in.citrus.fruit.by.reverse.phase.HPLC .

Thornton,. J..S..,. Olsen,. T..J. . and. Wagber,. K..,. Agr. . Food. Chem. . 25,. 573-576. (1977) . Determination. of. residues. of. metsystox-R. and. metabolite. in. Plant.and.animal.tissue.and.soil.

164

92

93

Определение.остаточных.содержаний.пестицидов:.рекомендуемые.методы.. CODEX.STAN.229-1993,.Rev..1-2003

Tjan,.G..H. .&.Konter,.Th..,.JAOAC,.54,.1122-1123.(1971).Gas-liquid.chroma- tography.of.Morestan.residues.in.plants .

80

Tuinstra,L. ..G..M..Th. &.Kienhuis,.P. ..G..M..,Chromatographia,.24,.696.-700(1987). . Automated. two-dimensional. HPLC. residue. procedure. for. glyphosate. on.cereals.and.vegetables.with .postcolumn.fluoregenic.labelling ..

158

VanHaver,.W..,.Z. .Lebensm. .Unters. .Forsch..,.172,.1-3.(1981) .Determination. of.carbendazim.and.thiophanate-methyl.residues.in.some.vegetables.and. fruits.by.highpressure.liquid.chromatography.

72, 77

VanWees,. A..M..P. . et. al..,. in:. Chromatography. and. Mass. Spectrometry. in. Nutrition.Science.and.Food .Safety,.A..Frigerio.&.H. .Milon.(edits..),. Elsevier,. Amsterdam,. Netherlands,. 19-25. A(1984). Chromatographic. methods.for.the.determination.of.inorganic.bromide.in.vegetables.

47

Veierov,.D. .&.Aharonson,.N..,.JAOAC,.63,.532-535.(1980) .Economic.method. for.analysis.of.fluid.milk.for.organochlorine.residues.at.the.10.ppb.level .

1 (not applicable to dieldrin), 12, 21, 43, 44, 48

Vuik,.J. .J. .Chromatogr. .553.299-304.(1991).Rapid.determination.of.abamectin. in.letluce.and.cucumber.by.high-performance.liquid .chromatography. ..

177

Wagner,. K. . and. Thornton,. J..S. . Pflanzensch. . Nachr. . Bayer,. 30. 1-17. (1977). Method. for. the. gas-chromatographic. determination. of. metasystox(i). and.Metasystox.R.residues.in.plants,.soil.and.water.(German.edit..:.30,. 1-17.(1977) .

73, 164, 166

Westcott. .N..D..,.J.Environm. .Science.and.Health.323,.317-330.(1988). .Terbufos. residues.in.wheat.and.barley. .

167

Wigfield,Y. ..Y. and.Lanquette,.M. . JAOAC,.74. . No. ..5,842.-847(1991). Residue.analysis.of. . glyphosateand.its.principal.metabolite.in.certain.cereals,.oilseeds.and.pulses.by. . liquid.chromatography.and.post-column.fluorescence.detection. ..

158

Winell,.B..,.Analyst,.101,.883-886.(1976) .Quantitative.determination.of.eth- oxyquin.in.apples.by.gas.chromatography.

35

Wright,.D..,.JAOAC.70,.718-720.(1987) .New.method.for.the.determination.of. 1,1-dimethylhydrazine.residues.in.apples.and.peaches .

104

Yamada,.T. .et.al..,.Agric. .Biol. .Chem..,.48,.1883-1885.(1984) .Determination.of. residual.thiabendazole.in.citrus.fruits.and.bananas.by.high.performance. liquid .chromatography.

65

Раздел.3. .Справочная.литература

Zimmerli,.B. .&.Marek,.B..,.Mitt. .Geb. .Lebensm. .Unters. .Hyg..,.63,.273-289. (1972).Entwicklung.einer.gaschromatographischen.Bestimmungs-.und. Bestдtigungsmethode. fьr. Hexachlorbenzolrьckstдnde. in. Fetten. und. Oelen.

44

Van. Zoonen,. P..,. E..A. . Hogendoorn,. D..C. . van. Harten,. Meded. . Fac. . Landbouwwetenschappen. Rijksuniversiteit. Gent,. 55. (3b),. 1285-1290. (1990) .Determination.of.fenpropimorph.residues.in.grains.by.LC.fol- lowed.by.confirmation.by.GC-MPD..

94

95